雪茄茄衣深度发酵过程中挥发性成分的变化

    Changes of Volatile Components in Cigar Wrapper During Deep Fermentation

    • 摘要:
      目的 目前尚不明确深度发酵对雪茄烟叶品质的影响,而挥发性成分是影响雪茄感官品质的重要因素,为探究茄衣深度发酵过程中挥发性成分的变化,分析深度发酵对雪茄烟叶品质的影响。
      方法 采用HS-SPME/GC-MS法对工业生产中雪茄茄衣深度发酵过程5个阶段的样品挥发性成分进行分析。
      结果 从茄衣样品中鉴定出37种挥发性成分,在种类上以含氮化合物和醇类为主,其次为酯类和酮类;在相对含量上以烟碱和新植二烯为主,其中挥发性烟碱相对含量最高、占挥发物总量的76.28%~83.32%,新植二烯占挥发物总量的11.60%~15.88%,其次为含氮化合物(除烟碱外)、酮类,挥发物整体呈显著上升趋势;从茄衣中筛选出主要差异挥发物13种,主要包括酮类的六氢假紫罗酮、香叶基丙酮、β-紫罗兰酮、植酮、法尼基丙酮,含氮化合物3-乙酰基吡啶、1-乙酰基吡咯烷、麦司明、二烯烟碱、2, 3’-联吡啶等。
      结论 深度发酵对茄衣中挥发物的种类无明显影响,但对其含量有明显影响。这将为雪茄烟叶品质的提高提供依据。

       

      Abstract:
      Objective At present, the effect of deep fermentation on the quality of cigar tobacco leaves is still unclear, and volatile components are important factors affecting the sensory quality of cigars. The study is carried out to explore the changes of volatile components during the deep fermentation of wrappers and to analyze the effects of deep fermentation on the quality of cigar tobacco leaves.
      Method HS-SPME/GC-MS method was used to analyze the volatile components of samples in five stages of deep fermentation of cigar wrappers in industrial production.
      Result 37 volatile components were identified from wrapper samples, mainly including nitrogen-containing compounds and alcohols, followed by esters and ketones. In terms of relative content, nicotine and neophytadiene were the main components. The relative content of volatile nicotine was the highest, accounting for 76.28% -83.32% of the total volatile matter, and that of neophytadiene accounted for 11.60% -15.88% of the total volatile matter, followed by nitrogen-containing compounds (except for nicotine) and ketones, and the volatiles showed a significant upward trend as a whole. 13 main differential volatile compounds were screened out from the wrappers, mainly including hexahydro pseudoviolone, geranyl acetone, β-ionone, phytone, farnesyl acetone, 3-acetylpyridine, 1-acetylpyrrolidine, mesamine, nicotyrine, and 2, 3'-bipyridine, etc.
      Conclusion Deep fermentation has no obvious effect on the types of volatiles in wrappers, but it has a significant effect on their contents. This will provide a basis for improving the quality of cigar wrappers.

       

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